Sitafloxacin_hydrate_LCMS_13362_MedChemExpress
Acq. Method : C:\Chem32\1\METHODS\1-POS-2MIN.M Analysis Method : C:\Chem32\1\METHODS\1-POS-2MIN.M Catalog No : HY-B0395C Batch#13362 Method Info : Mobile Phase: A: Water(0.01%TFA) B: ACN(0.01%TFA) Gradient: 5%B increase to 100%B within 0.8min,100%B for 1.1min. Flow Rate:1.5mL/min Column: Chromolith Fast Gradien RP-18e,50-3mm. Column Temperature: 40C Mass Range:100-1100
min*00.25
0.50.751 1.25 1.5 1.75mV
-0.1-0.05
0.05
*ADC1 A, ELSD
min*00.25
0.50.751 1.25 1.5 1.75mAU
-20
-10
*DAD1 A, Sig=214,4 Ref=off min*00.250.50.75
1 1.25 1.5 1.75mAU
5
*DAD1 B, Sig=254,4 Ref=off
min
00.25
0.50.751 1.25 1.5 1.75300000
400000
500000
600000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70,
0.417 Integration Results for ADC1 A, ELSD RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------|
Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------|
Integration Results for DAD1 B, Sig=254,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------|
m/z 20040060080010000
10000
20000
30000
40000
50000
60000
70000
80000
ES-API Positive
103.3 219.1 131.3 130.4
279.1 235.1 159.2 102.3 143.3
Acq. Method : C:\Chem32\1\METHODS\1-POS-2MIN.M Analysis Method : C:\Chem32\1\METHODS\1-POS-2MIN.M Catalog No : HY-B0395C Batch#13362 Method Info : Mobile Phase: A: Water(0.01%TFA) B: ACN(0.01%TFA) Gradient: 5%B increase to 100%B within 0.8min,100%B for 1.1min. Flow Rate:1.5mL/min Column: Chromolith Fast Gradien RP-18e,50-3mm. Column Temperature: 40C Mass Range:100-1100
min*00.25
0.50.751 1.25 1.5 1.75mV
-0.10
*ADC1 A, ELSD
min*
00.25
0.50.751 1.25 1.5 1.75mAU
1000
*DAD1 A, Sig=214,4 Ref=off 0.767min*00.250.50.75
1 1.25 1.5 1.75mAU
0100
*DAD1 B, Sig=254,4 Ref=off
0.767min 00.250.50.75
1 1.25 1.5 1.752000000
4000000
6000000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70,
0.779min
00.25
0.50.751 1.25 1.5 1.750
1000000
2000000
Ion 410, MSD1 410,Target Mass 409 +H Positive, EIC=409.7:410.7
0.778 Integration Results for ADC1 A, ELSD RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------|
Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 0.77 0.01 274.83 301.22 100.00
Integration Results for DAD1 B, Sig=254,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 0.77 0.01 245.60 265.52 100.00
m/z
20040060080010000
100000
200000300000
400000
500000
600000
700000
800000
ES-API Positive
159.2 413.1 101.2 157.2 411.2 410.2