论文中英文摘要

论文中英文摘要

作者姓名：义理林

论文题目：光分组交换网中的光信号处理技术研究

作者简介：义理林，男，1981年4月出生，2004年9月师从于上海交通大学大学胡卫生教授，于2008年6月获博士学位。

中文摘要

我国互联网国际出口总容量从2000年初的351Mbps增长到2006年初的136106Mbps，六年累计增加约430倍。网络带宽的增长，主要来源于数据业务的大幅度增长。未来的光网络将向融合分组化交换、支持多样性业务的、光电交换集成的、多颗粒带宽的、传送与交换融合的、安全高效的、灵活组网的方向发展。光分组交换网络（OPS）是光交换的理想模式，也是公认的光交换结构的终极发展目标。OPS的主要优点是带宽利用效率高，而且能提供各种服务，满足客户的需求。目的是把大量的交换业务转移到光域实现，从而实现交换容量与波分复用系统(WDM)的传输容量相匹配。OPS网络结构中的关键技术包括光开关、光逻辑、全光波长变换以及光缓存等多项技术。其中关开关是任何光交换网的核心功能器件，完成信号的交换和路由功能；光逻辑则完成信头检测处理重写等功能，用以实现未来的光控光交换；波长变换用于解决网络中的波长冲突，提高网络灵活性。光缓存是OPS网络必需的器件，用以实现数据包的存储功能，解决信号时间上的冲突；而以上所有的光信号处理都会导致信号的损耗，因此在OPS网络中，光放大器也必不可少，工作于OPS网络中的放大器还需具有宽带，以及增益控制的功能。只有上述各项技术全面成熟发展，才能推动OPS网络的快速发展，实现真正的全光交换网络。

本论文围绕全光分组交换网络中的关键技术研究开展了如下工作：

1．基于SOA/相位调制器的超快光开关

光开光是OPS网络的核心功能设备，一个大型的OPS网络需要大规模的超快光开关阵列。因此，超快（<1ns）以及易于扩展是设计光开关需要考虑的重要因素，同时成本也是不可忽略的另一个重要因素。

SOA和铌酸锂晶体可以支持快速的光开关操作，将SOA或者铌酸锂相位调制器（PM）放置于Sagnac干涉环中可以形成一个2×2的超快光开关，通过比较两者性能，我们最终选择PM-Sagnac干涉光开关。基于此PM-Sagnac干涉光开关首次实现了带组播功能的偏振无关2×2超快（<1ns）光开关操作，并在此基础上构建大型低成本超快光开关矩阵。

2．基于半导体光放大器（SOA）的可重构全光逻辑门以及波长变换

全光逻辑以及波长变换也是OPS网络的关键技术。波长变换用于解决网络拥塞造成的波长冲突，全光逻辑用以实现包头识别处理等功能。为了提高网络的灵活性，通常要求一个全光逻辑器件能实现多种逻辑功能，并且各逻辑操作结果的波长可根据需要进行调节以避免网络拥塞。

我们利用SOA的非线性偏振旋转效应（NPR）以及交叉增益调制效应（XGM）相结合实现了可重构全光逻辑门及波长变换，避免了以往基于干涉结构可重构逻辑门的高成本，以及基于四波混频效应（FWM）的可重构逻辑门对操作波长的限制。理论上基于单个SOA的NRR效应可实现所有逻辑操作（NOT，XOR，XNOR，OR，NOR，AND，NAND）。实验中，受器件的限制，我们实现了10-Gb/s数据的NOT，OR，NOR，AND，NAND逻辑操作以及同相波长变换（即变换后的信号和初始信号具有相同的极性）。

3．自动增益控制掺铒光纤放大器（AGC-EDFA）的设计

光开关以及逻辑操作都会造成信号功率的损耗，因此在OPS网络节点需要使用放大器补偿信号功率。此外，由于光分组的长度一般在几十微秒到几毫秒量级，与EDFA的铒离子能级驰豫时间相当，当某一波长光分组进入EDFA时会产生类似SOA中的XGM效应，影响其余信道上的光分组功率，因此工作于OPS网络中的EDFA还需具有增益控制的功能。同时考虑到OPS 网络对带宽的需求，我们分别设计了C波段增益控制EDFA和C＋L波段增益控制EDFA。

1）结合环形腔AGC-EDFA和反射型AGC-EDFA结构的优点，以低成本的方式解决了基于双光栅反射型AGC-EDFA中增益难以调谐的问题，并且采用双通结构提高增益效率。

2）设计了一个低噪声的并联式C＋L波段全光AGC-EDFA。1525nm-1610nm波长范围的信号都可得到有效放大，除了在1565nm-1572nm的“死区”外，所有波长的噪声指数都控制在约5.5dB的噪声水平。临界增益控制输入功率为-5dBm，在增益控制区内，增益变化小于0.2dB。4．基于宽带受激布里渊散射（SBS）的可调慢光延迟线性能研究

光缓存是OPS网络研究的重中之重，它的研究进展决定了OPS的实用进程。目前还没有可实用的光缓存，我们旨在通过减慢光速来实现信号的存储或者同步。基于SBS的慢光研究是目前的一大热点，我们的相关研究工作如下：

1）首次提出通过对布里渊泵浦进行相位调制来展宽布里渊放大器增益谱，将布里渊增益带宽展至1.6GHz，首次演示了1.25Gb/s 伪随机序列（PRBS）信号的在宽带SBS中的延迟，并比较了非归零（NRZ）和归零（RZ）脉冲的在此宽带SBS中的延迟性能。

2）进一步提出利用迈克－曾德强度调制器（MZM）替代相位调制器（PM）实现泵浦相位调制，展宽布里渊增益谱，可避免PM产生的相位调制信号具有的强时钟边带导致信号质量劣化的问题，从而可将布里渊增益谱展宽至10GHz。

3）在噪声直接调制展宽布里渊泵浦的情况下，使用一高功率电放大器将高斯电噪声放大至饱和，此时能量主要集中在中心的高斯噪声将变成能量均匀分布的超高斯噪声。超高斯噪声调制产生的布里渊泵浦以及对应的布里渊增益谱也呈超高斯分布，因此在相同的布里渊泵浦功率下，相对高斯噪声调制情况，超高斯分布的泵浦将获得更大的布里渊增益，亦即更大的慢光延迟量。

4）首次采用具有高谱效率，抗色散性强的10Gb/s双二进制（Duobinary）信号作为布里渊信号在宽带SBS中进行延迟，与10Gb/s的NRZ信号进行比较，可避免慢光色散以及滤波效应带来的信号劣化，从而大幅度提高延迟后的信号质量，具体表现为延迟后的接收灵敏度得到有效提高。

5）首次利用带宽可调的高斯型SBS增益实现了任意比特速率DPSK信号的同时延迟和解调，并基于此获得了创记录的10Gb/s信号无误码延迟性能（最大无误码延迟时间为81.5ps）。5．基于光纤参量放大（FOPA）的可调慢光延迟线

相对SBS慢光，基于FOPA的慢光延迟线主要优点在于带宽更大，可支持更高速率（如160Gb/s）的信号延迟；另外，参量噪声低于布里渊放大，因此延迟导致的信号质量劣化更小。

1）理论推导了基于参量效应的慢光表达式，利用窄带（带宽约1.6nm）光纤参量放大实现可调慢光延迟，通过改变泵浦波长或光纤的零色散波长，实现整个通信波段（C＋L波段）信号的可控延迟。

2）用10Gb/s RZ数据包代替单个信号脉冲进行延迟演示，首次演示了无误码慢光操作，50ps宽脉冲延迟15ps灵敏度代价仅为0.6dB，从系统的高度验证了参量可调慢光延迟线的用于实际系统的可行性。

关键词：全光网光分组交换网掺铒光纤放大器受激布里渊散射光纤参量放大半导体光放大器慢光光逻辑波长变换光开关

The research on optical information processing technologies in optical

packet switching networks

Lilin Yi

ABSTRACT

In China, from 2000 to 2006, the exporting amount of the Internet data has been increased from 351Mbps to 136106Mbps, and the increasing ratio is about 6 times within 6 years. The increase of network bandwidth mainly comes from the quickly increasing of the data service. In the future, the optical network will develop towards packet switching, supporting versatile services, integrated switching of optics and electronics, merging of transmission and switch, security and efficiency, flexible networking etc. Optical packet switching is the ideal switching mode, and it is also recognized as the final goal of optical switching configuration. The main advantages of OPS include high bandwidth efficiency and providing all kinds of services so as to meet different customers’requirements. The purpose of the OPS network is transferring large amount of switching services from electrical to optical domain so as to match the switching capabilities of OPS network with the transmission capabilities of wavelength division multiplexing (WDM) system. The key technologies in the OPS network include optical switch, optical logic operation, wavelength conversion and optical buffer etc. The optical switch is the core functional component of OPS networks, which is used to realize the switching and routing of signals. The optical logic operation can be used to detect, process and rewrite of the labels, which is expected to realize the future optically controlled optical switch. The function of wavelength conversion is to solve the wavelength conflict of the network and improve the flexibility of the network. The most important and indispensable component in OPS network is the optical buffer, which is used for storing the data packet to solve the time conflict of signals. Furthermore, all the components described above induce signal loss, therefore in OPS networks, optical amplifiers are mandatory used. The optical amplifiers working in OPS networks should feature the function of broad bandwidth and gain clamping. Only all the technologies are fully developed, the truly all-optical network can be realized. For accelerating the development of OPS networks, our thesis focus on the researches of the key technologies as follows:

1．SOA and phase modulator(PM)-Sagnac interferometer based ultra-fast optical switch Optical switch is the core functional component of the OPS network. Normally, an OPS network requires a large scale and ultra-fast optical switch matrix, therefore ultra-fast (

A 2×2 ultra-fast optical switch with low cost can be constituted by putting an SOA or a LiNbO3 phase modulator (PM) inside a Sagnac interferometer, and the performance of the latter one is better in comparison. Based on the PM-Sagnac interferometer, a multi-casting supported, polarization-insensitive 2×2 ultra-fast (<1ns) optical switch with low cost is demonstrated for the first time. The 2×2 optical switch is easy to be extended into a large scale ultra-fast optical switch matrix, which is very useful in future optical networks.

2．Semiconductor optical amplifier (SOA) based on reconfigurable all-optical logic gate and wavelength converter

All-optical logic operation and wavelength conversion are the key technologies in the OPS

network. Wavelength conversion is used to solve the wavelength conflict due to the data traffic jam and all-optical logic operation is used for recognizing and processing the label of packets. To improve the flexibility of the optical network, it is desired that an optical logic gate can realize multiple logic operations, which is called a reconfigurable logic gate, and the wavelength of logic operation can flexibly tuned according to the practical requirements for avoiding the network data jam.

Utilizing the nonlinear polarization rotation (NPR) and the cross-gain modulation (XGM) effects of the SOA, reconfigurable logic operation and wavelength conversion can be realized. We experimentally demonstrate reconfigurable NOT, OR, NOR, AND, and NAND logic operations and non-inverted wavelength conversion with a 10-Gb/s bit rate based a single SOA.

3．Design of all-optical gain-clamped erbium-doped fiber amplifier (GC-EDFA) Both optical switch and logic gate induce power loss; therefore an optical amplifier is required for compensating the power loss. Moreover, the packet length is normally several tens of micro seconds or several milliseconds, which is comparable with the response time of the erbium level. When the optical packets in one channel are sent into the EDFA, the XGM effect will be induced like the SOA case, which affects the packet power in other channels. Therefore the EDFAs working in the OPS network require gain-clamping performance, which means the signal gain is independent with the input signal power. Considering the bandwidth requirement of the OPS network, we designed a conventional band (C-band) gain-clamped EDFA and a C-band plus long-wavelength (L-band) EDFA as follows:

1）Combining the advantages of the ring-cavity GC-EDFA and the reflexible GC-EDFA, we solve the problem that the clamped-gain is very difficult to tune in the conventional reflexible GC-EDFA constituted by two fiber Bragg gratings. And the gain efficiency is improved through a double-pass configuration.

2）We design a parallel C+L band GC-EDFA with low noise figure (NF). The signal can be effectively amplified in the wavelength range from 1525nm to 1610nm. Within the range, the NF can be controlled at about 5.5dB except for the “dead zone” from 1565nm to 1572nm. The dynamic gain-clamped range of the input signal power is up to -5 dBm, and the variation of the clamped-gain are lower than 0.2 dB within it.

4．Broadband stimulated Brillouin scattering (SBS) based slow-light delay line Optical buffer is the most important part in the OPS network. Its research progress determines whether the OPS network can be put into practical applications. Until now, there is no practical optical buffer. In our case, we try to realize data storage or packet synchronization by slowing down the group velocity of light. At present, Stimulated Brillouin Scattering (SBS) based slow light has been attracted much interest, and our research achievements in this topic are presented as follows: 1）The SBS gain bandwidth is broadened to 1.6GHz through phase-modulating the Brillouin pump laser with a 2.5-Gb/s bit rate. Based on the broadened SBS gain, the tunable slow-light delay of 1.25-Gb/s non-return-to-zero (NRZ) and return-to-zero (RZ) pseudorandom bit sequence (PRBS) data is experimentally demonstrated. The delay performance of the RZ data is better than the NRZ case, and the corresponding delay can exceed one bit-duration.

2）We further proposed that using a Mach-Zehnder modulator (MZM) to take place the phase modulator for broadening the Brillouin pump spectrum can avoid the signal degradation due to the strong clock components induced by the phase modulator, so as to improve the gain bandwidth to about 10GHz and support the time delay of 10-Gb/s signal.

3）In the case of the direct noise modulation of the laser diode, a high power electrical amplifier can amplify the Gaussian noise to saturation, which makes the energy evenly distribute at the center of the optical spectrum, therefore the Gaussian noise becomes super-Gaussian one. Super-Gaussian noise modulation of the pump LD generates a super-Gaussian shaped pump

spectrum and SBS gain. Compared with the Gaussian one, the super-Gaussian shaped pump spectrum induces larger SBS gain value, resulting in larger time delay.

4）Through direct-modulation of the Brillouin pump laser using a super-Gaussian noise, the SBS gain bandwidth can be further broadened to about 10GHz. Based on the broadband SBS, the tunable delay with good performances of a 10-Gb/s Duobinary signal is experimentally demonstrated. Compared with the 10-Gb/s NRZ case, the signal quality after delay is much improved owing to the high spectral efficiency and strong dispersion-tolerance of the Duobinary signal, which can suppress the SBS filtering effect and the dispersion accompanied with slow light. After a 35-ps delay, the sensitivity of the Duobinary signal is improved about 2dB compared with the back-to-back case, and the maximal delay with error-free operation is 50ps.

5）A bandwidth-tunable SBS gain with Gaussian-shape is proposed to simultaneously delay and demodulate differential phase shift keying (DPSK) signals with any bit-rate. We experimentally demonstrate the demodulation with high sensitivities and the large fractional delay of 10-Gb/s and 2.5-Gb/s DPSK signals. For the 10-Gb/s DPSK signal, the maximal delay with error-free operation is 81.5ps, which is the best record in all the 10-Gb/s slow light demonstrations.

5．Fiber optical parametric amplification (FOPA) based slow-light delay line Compared with the SBS based slow light, FOPA based slow light features larger gain bandwidth, which can support the time delay of higher data rate such as 160Gb/s. Furthermore, owing to the low noise of the parametric process, the slow-light induced signal degradation is much lower than that in the SBS case. Our work in this topic is as follows:

1）The delay expression of FOPA based slow light is derived. Utilizing the narrow bandwidth (~1.6nm) of the FOPA, and optimizing the pump wavelength and the zero-dispersion wavelength of the fiber, the tunable delay of the signals in entire telecommunication waveband (C+L band) can be realized.

2）For the first time, the slow light with error-free operation is experimentally demonstrated using a 10-Gb/s RZ data packet transmitted in a narrow-band FOPA. The sensitivity penalty is only 0.6dB for a 15-ps delay, which proves that the FOPA based slow light is suitable for practical applications.

Key words: all-optical network, optical packet switching (OPS), erbium-doped fiber amplifier (EDFA), stimulated Brillouin scattering (SBS), fiber optical parametric amplification (FOPA), semiconductor optical amplifier (SOA), slow light, optical logic gate, wavelength conversion, optical switch.

英语毕业论文最新英文论文的致谢词

最新英文论文的致谢词 论文英文答谢词1 First of all, I would like to extend my sincere gratitude to my supervisor, Zhang Hong, for her instructive advice and useful suggestions on my thesis. I am deeply grateful of her help in the completion of this thesis. High tribute shall be paid to Ms. Geng Li, whose profound knowledge of English triggers my love for this beautiful language and whose earnest attitude tells me how to learn English. I am also deeply indebted to all the other tutors and teachers in Translation Studies for their direct and indirect help to me. Special thanks should go to my friends who have put considerable time and effort into their comments on the draft. Finally, I am indebted to my parents for their continuous support and encouragement. 论文英文答谢词2 I would like to express my gratitude to all those who helped me during the writing of this thesis.

毕业论文中英文摘要及目录(供参考)

密级：立体停车库的PLC控制系统设计 Design of PLC Control System for Parking Garage 学院： 专业班级： 学号： 学生姓名： 指导教师： 2018年6月

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毕业论文摘要格式

毕业论文摘要格式 论文摘要是文章的内容不加诠释和评论的简短陈述。为了国际交流,还应有外文(多用英文)摘要。摘要是在文章全文完成之后提炼出来的,具有短、精、完整三大特点。摘要应具有独立性的自含性、即不阅读原文的全文.就能获得必要的信息。摘要中有数据、有结论、是一篇完整的短文.可以独立使用,也可以引用,还可以用于工艺推广。其内容应该包含与报告论文同等量的主要信息.以供读者确定有无必要阅读原论文全文,也可提供给文摘第二次文献采用。摘要一般应说明研究工作目的、实验方法、结果和最终结论等.而重点是结果和结论。中文摘要一般不宜超过300字,外文摘要不宜超过250个实词。除了实在迫不得已,摘要中不用图、表、化学结构式、非公知公用的符号和术语。摘要可用另页置于题名页(页上无正文)之前,学术论文的摘要一般置于题名和作者之后,论文正文之前。 论文摘要又称概要、内容提要。摘要是以提供文献内容梗概为目的,不加评论和补充解释,简明、确切地记述文献重要内容的短文。其基本要素包括研究目的、方法、结果和结论。具体地讲就是研究工作的主要对象和范围,采用的手段和方法,得出的结果和重要的结论,有时也包括具有情报价值的其它重要的信息。摘要应具有独立性和自明性,并且拥

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要 随着时代的发展，人们对纺织品的要求也已经不再仅仅局限于实用。激烈的国际竞争逼使纺织企业采用高新 技术重视绿色工艺，开发环保产品则已成为新世纪市场竞争的新焦点。欧共体的Eco-label 倡导的是全生态的概念，欧盟委员会（2002/371/EC ）生态标准中，在纺织纤维中列出腈纶纤维的考核指标：原料纤维中丙烯腈的残留量应低于1.5mg/kg 。 丙烯腈是一种有毒物质，且有致癌作用。其极毒，对温血动物的毒性约为氰化氢的1/30。丙烯腈不仅蒸气有毒，而且附着于皮肤上也易经皮肤中毒。长时间吸入稀丙烯腈蒸气，则能引起恶心、呕吐、头痛、疲倦和不适等症状。由此可见，丙烯腈直接危害着人们的健康。 本文依照欧盟（2002/371/EC ）生态标准对腈纶纤维中丙烯腈残留量的控制，通过试验论证，确立了采用顶空固相微萃取和色质联用技术（HS —SPME —GC/MS ），由此建立腈纶纤维中丙烯腈残留量的测定方法。该方法具有操作简单，便捷，灵敏度高，准确性好的优点，而且仪器价格适中，便于推广。本文实验所使用的方法检测限低于0.5mg/kg ，回收率在86.2～ 关键词：腈纶，丙烯腈，残留量，气相色谱/质谱

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2021年毕业论文致谢词中英文范例

毕业论文致谢词中英文范例 acknowledgements my deepest gratitude goes first and foremost to professor aaa , my supervisor, for her constant encouragement and guidan ___. she has walked me through all the stages of the writing of this thesis. without her consistent and illuminating instruction, this thesis could not havereached its present form. second, i would like to express my heartfelt gratitude to professor aaa, who led me into the world of translation. i am also greatly indebted to the professors and teachers at the department of english: professor dddd, professor ssss, who have instructed and helped me a lot in the past two years. last my thanks would go to my beloved family for their loving considerations and great confiden ___ in me all through these years. i also owe my sin ___re gratitude to my friends and my fellow class ___tes who gave me their

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毕业设计（论文） 新民本主义： 传统民本思想与现代民主理念的契合（字体:黑体小一） 专业年级 学生学号 学生姓名 指导老师 评阅人 二○○年月 中国·南京

摘要 （“摘要”两字的字体为黑体三号,居中。） 正文字体均为：宋体小四号，行距为倍 （不低于400字） 关键词：民本；民主；新民本主义 （“关键词”三字字体为黑体，内容(3-5)个，宋体小四号。各关键词之间用；）注意：摘要和关键词只能单独一页.

Abstract （“Abstract”一词用Times New Roman字体三号,加黑,居中。） Thought of people as the center is the marrow of our traditional culture and the core of the theory of managing state affairs. It germinates in the early state of antiquity society and is based on patriarchal clan system. It is also a kind of value seeking for the realization of the ethic reason and moral justice. Its basic thinking is that the monarch is defined by people and conversely people are defined by the monarch. At first appearance, its purpose is to value people’s suffering,fate and interest on the ruler’s position. However, its real intention is to fool the people so as to strengthen and consolidate the ruler’s rule. The theory of “people-oriented concept” includes nine topics such as “the theory of people is being the root of the monarch’s rule”, “the theory of people is being more valuable than the monarch”, “the theory of the monarch is being people’s servant”and so on. People –oriented means “value the people ”in essence, which sees “people”as its foundation of politics rule, ranking official, and administration. （正文字体为：Times New Roman字体，小四号，且行距为单倍或倍。） Key words：people- oriented concept；democracy；new people-basisism （“K ey words”一词用Times New Roman字体小四号,加黑。） 注意：英文摘要和关键词只能单独一页.

【开题报告】毕业论文“英、中文摘要、关键词”样式

毕业论文“英、中文摘要、关键词”样式abstract this paper begins with a brief introduction to chomsky’s methodology of idealization in linguistic research. although the idealization in physical research from which chomsky’s idealization deprives can still keep natural laws’ validity, the author points out chomsky’s idealization is not accessible. the key point lies in the exclusion of social factors in his research. then the author demonstrates the reason why chomsky’s exclusion of social factors is not accessible from two aspects: (1) language is a concrete system of signs. (2)language is a social institution. only in the context of society are these features significant and integrate, can language bear its form and forward its development and keep up the interaction with the society. therefore instead of “being idealized” out of linguistic research, social factors should be regarded as the base of the research. otherwise the object of the research will be totally changed and the research itself will be misguided. as for what factors can be temporarily idealized without changing language’s fundamental features? this is a question worth our further study in the future. 摘要：本文从chomsky在语言学研究过程中所采用的理想化模式入手，认为chomsky为了使研究变得简单，便将与语言关系紧密的社会因素摒除在研究范围之外，这是一种不可取的理想模式。接下来本文从两个主要方面阐述了理想化模式不可取的原因：一是语言作为一种符号系统，只有在社会的环境下才能具有完整的意义。二是语言作为一种社会结构，无论是它的产生还是发展过程，都在不断地和社会发生着相互作用。故而只要是研究语言学，我们就不能将社会因素“理想化”。至于什么因素可以暂时不予考虑，这仍有待进一步的研究。 1 / 1

论文中英文摘要格式

论文中英文摘要格式

附件2 作者姓名：顾振华 论文题目：2,3-联烯酸(酰胺)与联烯和炔烃的偶联环化反应研究 作者简介：：顾振华，男，1979年02月出生，2002年09月师从于中国科学院上海有机化学研究所麻生明教授，于2007年7月获博士学位。 中文摘要

联烯是一类含有1,2-丙二烯官能团的化合物。在联烯的三个碳原子中，末端的两个sp2杂化的碳原子以剩下的未杂化的p轨道与中间的sp杂化的碳原子的两个互相垂直的p-轨道交盖形成两个互相垂直的π轨道。当联烯末端的同一碳原子上的取代基两两不同时，联烯则具有轴手性，其构型可通过Cahn-Ingold-Prelog规则判定。联烯化合物独特的反应性一方面来自这种独特的互相垂直交盖π-轨道，另一方面来自联烯末端的两个碳原子（四个取代基）对不同取代基的装载能力。通过对底物及反应条件的调控，反应可以选择性的发生在联烯的三个不同的碳原子上。由于其独特的结构及反应性，联烯在天然产物的合成中也有比较广泛地应用。近年来越来越多的含联烯结构的天然产物被分离和鉴定，到目前为止已有约150个，这也极大地推动了联烯化学的发展。 我们小组在官能化的联烯的环化反应方面也作了一些研究。最近我们小组发现并发展了官能化联烯的双分子氧化偶联反应，该反应能有效的一步构建双环化合物。基于这些发现，我的工作就是设计和发展联烯与联烯、联烯与炔烃的偶联环化反应。主要包括以下三大部分：第一部分：2,3-联烯酸(酰胺)与联烯的偶联环化反应 1．我们研究了2,3-联烯酸双分子氧化偶联反应。在研究过程中我们发展了三套氧化体系(a) n-C3H7I + O2, (b) KI + O2, (c) 苯醌来实现钯物种的催化循环，并且还研究了 在这三套氧化体系下的取代基效应。 2．在实现了2,3-联烯酸自身双分子氧化偶联反应之后我们又研究了2,3-联烯酰胺与1,2-联烯基酮的交叉偶联反应。根据我们小组以前的研究2,3-联烯酰胺有两种环化方 式：即氧进攻生成Furanimine结构的化合物，或氮进攻生成内酰胺的产物。通过 X-射线单晶衍射和核磁研究，我们确认了在这一双分子氧化偶联反应中联烯酰胺的 关环方式是氧进攻生成Furanimine结构的化合物，并且产物亚胺部分的结构是顺式 的。同时我们还观察到了2,3-联烯酰胺自身双分子偶联环化后部分水解的产物。 (a)来自亲核试剂进攻碘鎓三元环时的立体位阻效应。这是少数几例非杂原子导向的 高选择性羟碘化反应。 (b)我们还初步研究了β-联烯基呋喃酮的γ-羟基化反应。在有氧和碱性条件下，2(5H)- 呋喃酮能发生γ-羟基化反应生成5-羟基2(5H)-呋喃酮。当底物是β-联烯基呋喃酮时，γ-羟基化产物在I2存在下能有效的发生碘环化反应，有效地构建了双环化合物。 (c)我们发现了1,2,4(Z),7-四烯(α-烯丙基-β-联烯基呋喃酮)异构环化成八元环的反 应。该反应操作非常简单，只要将1,2,4Z,7-四烯在二甲苯中100 o C搅拌反应6小时 即可，产率高达98%。当向体系中加入亲双烯体，如马来酰胺时我们能得到一系列 结构新颖的桥环化合物，反应的立体选择性是单一的，即亲双烯体是以endo方式